CHEMICAL EFFECTS OF DCCA TO THE SOL-GEL REACTION PROCESS

被引:53
作者
UCHIDA, N
ISHIYAMA, N
KATO, Z
UEMATSU, K
机构
[1] Department of Chemistry, Nagaoka University of Technology, Nagaoka
关键词
D O I
10.1007/BF01151115
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The effects of drying control chemical additives (DCCA) on the growth of silica particles, gelation time and physical properties of the dry gel were examined in a two-step silica sol-gel process. N,N-dimethylformamide, N,N-dimethylacetamide and ethylene glycol (EG) were applied as DCCAs. The shapes of growing silica particles were distorted spheres on addition of DCCA. EG accelerated the gelation process. Despite the use of DCCA, crack-free, dry gels were obtained only under limited conditions.
引用
收藏
页码:5188 / 5192
页数:5
相关论文
共 8 条
[1]   PREPARATION OF MONOLITHIC SILICA-GEL AND GLASS BY THE SOL-GEL METHOD USING N,N-DIMETHYLFORMAMIDE [J].
ADACHI, T ;
SAKKA, S .
JOURNAL OF MATERIALS SCIENCE, 1987, 22 (12) :4407-4410
[2]   SINTERING OF SILICA-GEL DERIVED FROM THE ALKOXYSILANE SOLUTION CONTAINING N,N-DIMETHYLFORMAMIDE [J].
ADACHI, T ;
SAKKA, S .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1988, 100 (1-3) :250-253
[3]   EFFECT OF HYDROLYTIC POLYCONDENSATION OF TETRAETHOXYSILANE ON SPECIFIC SURFACE-AREA OF SIO2 GELS [J].
BOONSTRA, AH ;
MULDER, CAM .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1988, 105 (03) :201-206
[4]   SOL-GEL TRANSITION IN SIMPLE SILICATES [J].
BRINKER, CJ ;
KEEFER, KD ;
SCHAEFER, DW ;
ASHLEY, CS .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1982, 48 (01) :47-64
[5]  
Hench L. L., 1984, SCI CERAMIC CHEM PRO, P52
[6]   THE SOL-GEL PROCESS [J].
HENCH, LL ;
WEST, JK .
CHEMICAL REVIEWS, 1990, 90 (01) :33-72
[7]  
Wallace S, 1984, MATER RES SOC S P, V32, P47, DOI 10.1557/PROC-32-47
[8]  
ZARZYCKI J, 1987, ULTRASTRUCTURE PROCE, P27