SUBSTOICHIOMETRIC DETERMINATION OF PALLADIUM BY NEUTRON ACTIVATION ANALYSIS

被引：8

作者：

DOCTOR, ZK

HALDAR, BC

机构：

[1] Inorganic and Nuclear Chemistry Laboratory, Institute of Science

来源：

JOURNAL OF RADIOANALYTICAL CHEMISTRY | 1969年 / 3卷 / 5-6期

关键词：

D O I：

10.1007/BF02513785

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A method is described for the substoichiometric determination of traces of palladium by neutron activation analysis involving the extraction of palladium with isonitrosoacetophenone. The sensitivity of the method is 0.005 μg of Pd. With 200 mg of silver alloy containing 0.0005% palladium, the average of three determinations of Pd is 0.98 μg, which varies between 1.07 μg and 0.91 μg at 95% confidence limit. The time required for radiochemical purification and counting of the sample does not exceed 12 minutes. © 1969 Akadémiai Kiadó.

引用

页码：405 / &

共 7 条

[1]

BROWN H, 1948, AECD2296

[2]

KILICK RA, 1961, TALANTA, V8, P601

[3] SUBSTOICHIOMETRIC DETERMINATION OF TRACES OF MOLYBDENUM BY NEUTRON ACTIVATION ANALYSIS [J].