PREPARATION OF AROMATIC IODOACETYL DERIVATIVES BY DIRECT IODINATION WITH A POTASSIUM-IODIDE POTASSIUM IODATE SULFURIC-ACID SYSTEM

被引：26

作者：

OKAMOTO, T

KAKINAMI, T

NISHIMURA, T

IRWANHERMAWAN

KAJIGAESHI, S

机构：

[1] YAMAGUCHI UNIV, FAC ENGN, DEPT APPL CHEM & CHEM ENGN, UBE, YAMAGUCHI 755, JAPAN

[2] UBE TECH COLL, DEPT CHEM & BIOL ENGN, UBE 755, JAPAN

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN | 1992年 / 65卷 / 06期

关键词：

D O I：

10.1246/bcsj.65.1731

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of aromatic acetyl derivatives with potassium iodide and potassium iodate in acetic acid in the presence of sulfuric acid at room temperature gave iodoacetyl derivatives in good yields.

引用

页码：1731 / 1733

页数：3

共 20 条

[1]

BACKER JW, 1932, J CHEM SOC, P1148

[2]

BAKER JW, 1931, J CHEM SOC, P2416

[3]

BARLUENGA J, 1986, SYNTHESIS-STUTTGART, P678

[4] OXIDATION OF OLEFINS WITH SILVER CHROMATE-IODINE - NEW AND FACILE SYNTHESIS OF ALPHA-IODO KETONES [J].

CARDILLO, G ;

SHIMIZU, M .

JOURNAL OF ORGANIC CHEMISTRY, 1977, 42 (26) :4268-4270

[5]

COLLET A, 1990, B SOC CHIM FR, V23, P829

[6]

CORT AD, 1991, J ORG CHEM, V56, P6708

[7] PYRIDINIUM DICHROMATE IN ORGANIC-SYNTHESIS - A CONVENIENT OXIDATION OF OLEFIN-IODINE COMPLEXES TO ALPHA-IODO KETONES [J].

DASCOLI, R ;

DAURIA, M ;

NUCCIARELLI, L ;

PIANCATELLI, G ;

SCETTRI, A .

TETRAHEDRON LETTERS, 1980, 21 (47) :4521-4522

[8] ALPHA-IODOKETONES .2. REACTION OF ENOL ACETATES WITH N-IODOSUCCINIMIDE [J].

DJERASSI, C ;

LENK, CT .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1953, 75 (14) :3493-3495

[9]

EVANS RD, 1986, SYNTHESIS-STUTTGART, P727

[10] STUDIES IN THE SYNTHESIS OF CORTISONE .18. THE PREPARATION OF CORTISONE ESTERS FROM 4-5-ALPHA-DIHYDROCORTISONE [J].

EVANS, RM ;

HAMLET, JC ;

HUNT, JS ;

JONES, PG ;

LONG, AG ;

OUGHTON, JF ;

STEPHENSON, L ;

WALKER, T ;

WILSON, BM .

JOURNAL OF THE CHEMICAL SOCIETY, 1956, (NOV) :4356-4368

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