This paper describes the methodology for the preparation of self- supporting hollow diamond helix and diamond sieve in addition to diamond microtubes. The key idea is to deposit thick, compact and sufficiently strong coating on a suitable mandrel and then dissolve the latter so as to form the required shape. For this purpose we have made use of 'jet-flow' HFCVD which allows diamond deposition over larger area on three dimensional substrates both inside as well as outside. X-ray diffraction, laser macro-Raman spectroscopy and scanning electron microscopy have been used to characterise shape, morphology and the phase purity of the material.