GAS CHROMATOGRAPHY OF EPOXYGLYCERIDES

被引：14

作者：

FIORITI, JA

KANUK, MJ

SIMS, RJ

机构：

[1] General Foods Corporation, Technical Center, White Plains, NY

来源：

JOURNAL OF CHROMATOGRAPHIC SCIENCE | 1969年 / 7卷 / 07期

基金：

美国国家卫生研究院;

关键词：

D O I：

10.1093/chromsci/7.7.448

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Epoxyglycerides react with ketones in the presence of baron trifluoride to give 1,3-dioxolane derivatives. These derivatives are useful in the separation and identification of epoxyglycerides by gas liquid chromatography. Cyclopentanone is the most suitable reagent since it gives a derivative which has a large separation factor from the long-chain common triglycerides. The analysis of epoxyglyceride mixtures by GLC as their 1,3-dioxolane derivatives is described. © 1969, Oxford University Press. All rights reserved.

引用

页码：448 / &

共 11 条

[1] OPTICAL AND GEOMETRIC ISOMERS OF SOME FATTY ACIDS WITH VICINAL HYDROXY GROUPS
EWING, DF
HOPKINS, CY
[J]. CANADIAN JOURNAL OF CHEMISTRY-BACK YEAR, 1967, 45 (11): : 1259 - +
[2] FIORITI JA, IN PRESS
[3] STUDIEN AUF DEM FETTGEBIET .230. UBER C-18-POLYHYDROXY-FETTSAUREN UND C-18-POLYHYDROXY FETTALDEHYDE
KAUFMANN, HP
JANSEN, H
[J]. CHEMISCHE BERICHTE-RECUEIL, 1959, 92 (11): : 2789 - 2797
[4] KUESTER FE, 1964, Patent No. 3127418
[5] GAS-LIQUID CHROMATOGRAPHY OF TRIGLYCERIDE MIXTURES CONTAINING BOTH ODD AND EVEN CARBON NUMBER FATTY ACIDS
LITCHFIELD, C
HARLOW, RD
REISER, R
[J]. LIPIDS, 1967, 2 (05) : 363 - +
[6] QUANTITATIVE GAS-LIQUID CHROMATOGRAPHY OF TRIGLYCERIDES
LITCHFIELD, C
HARLOW, RD
REISER, R
[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1965, 42 (10) : 849 - +
[7] SYNTHESIS OF VINYL THREO-9 10-THREO-12 13-TETRAHYDROXYSTEARATES
ODONNELL, JL
GAST, LE
COWAN, JC
DEJARLAI.WJ
MCMANIS, GE
[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1967, 44 (11) : 652 - &
[8] TALLENT WH, 1966, J LIPID RES, V7, P531
[9] TALLENT WH, 1968, J LIPID RES, V9
[10] GLC AND TLC ANALYSIS OF ISOPROPYLIDENE DERIVATIVES OF ISOMERIC POLYHYDROXY ACIDS DERIVED FROM POSITIONAL AND GEOMETRICAL ISOMERS OF UNSATURATED FATTY ACIDS
WOOD, R
[J]. LIPIDS, 1967, 2 (03) : 199 - &

← 1 2 →