CONTINUOUS SOLVENT-EXTRACTION IN A CLOSED-LOOP SYSTEM

被引:33
作者
ATALLAH, RH [1 ]
RUZICKA, J [1 ]
CHRISTIAN, GD [1 ]
机构
[1] UNIV WASHINGTON, DEPT CHEM, CTR PROC ANALYT CHEM, BG 10, SEATTLE, WA 98195 USA
关键词
ORGANIC COMPOUNDS - ZINC COMPOUNDS;
D O I
10.1021/ac00151a015
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An on-line continuous-flow solvent extraction system has been developed. The method consists of a segmentor, an extraction coil, a phase separator, a switching valve, and a pumping system. The performance of the system was illustrated by extracting copper with a solution of zinc diethyldithiocarbamate in chloroform. Parameters affecting proconcentration of the analyte in the system were examined. The method can be used for quantitative analysis and as a preparative technique.
引用
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页码:2909 / 2914
页数:6
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