SOLID-STATE CONFORMATIONS OF 4 TRUXILLIC AND TRUXINIC DIAMIDES

被引：2

作者：

CACCAMESE, S ^{[1
]}

FRONCZEK, FR ^{[1
]}

机构：

[1] LOUISIANA STATE UNIV,DEPT CHEM,BATON ROUGE,LA 70803

来源：

TETRAHEDRON | 1990年 / 46卷 / 23期

关键词：

D O I：

10.1016/S0040-4020(01)90081-X

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Solid-state conformations were determined by crystal structural analyses in α- and ε-truxilloyldiamides and β- and δ-truxinoyldiamides (compounds 1-4) where each cyclobutyl carbon brings an independent substituent. While the cyclobutane ring of the virtual centrosymmetric 1 is slightly non-planar, with unusual bonds and angles values, that of all other three compounds is folded, with puckering angles up to 31°. © 1990.

引用

收藏

页码：7841 / 7848

页数：8

相关论文

共 21 条

[1] THE GEOMETRY OF SMALL RINGS .6. GEOMETRY AND BONDING IN CYCLOBUTANE AND CYCLOBUTENE [J].

ALLEN, FH .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1984, 40 (FEB) :64-72

[2] X-RAY STRUCTURE DETERMINATION OF CYCLOBUTANE PHOTODIMERS FROM (Z)-ALPHA, BETA-DIARYLACRYLONITRILES [J].

AMATO, ME ;

MUSUMARRA, G ;

SCARLATA, G ;

LAMBA, D ;

SPAGNA, R .

JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH, 1989, 19 (05) :791-808

[3] The photochemical dimerization of trans-cinnamic acid [J].

Bernstein, HI ;

Quimby, WC .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1943, 65 :1845-1846

[4]

BUTENANDT A, 1952, LIEBIGS ANN CHEM, V575, P123

[5] RETENTION BEHAVIOR OF DIASTEREOMERIC TRUXILLIC AND TRUXINIC DIAMIDES AND SEPARATION OF AN ENANTIOMERIC PAIR IN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

CACCAMESE, S .

JOURNAL OF CHROMATOGRAPHY, 1988, 457 :366-371

[6] REVISION OF STEREOCHEMICAL ASSIGNMENT OF A CYCLOBUTANE DERIVATIVE FROM CHALCONE PHOTO-DIMERIZATION VIA X-RAY-DIFFRACTION ANALYSIS [J].

CACCAMESE, S ;

MCMILLAN, JA ;

MONTAUDO, G .

JOURNAL OF ORGANIC CHEMISTRY, 1978, 43 (13) :2703-2704

[7] PHOTODIMERS OF CINNAMIC ACID AND RELATED COMPOUNDS - STEREOCHEMICAL STUDY BY ELECTRON-IMPACT AND FIELD DESORPTION MASS-SPECTROMETRY [J].

CACCAMESE, S ;

MONTAUDO, G ;

PRZYBYLSKI, M .

ORGANIC MASS SPECTROMETRY, 1974, 9 (11) :1114-1123

[8] TOPOCHEMISTRY .2. PHOTOCHEMISTRY OF TRANS-CINNAMIC ACIDS [J].

COHEN, MD ;

SCHMIDT, GMJ ;

SONNTAG, FI .

JOURNAL OF THE CHEMICAL SOCIETY, 1964, (JUN) :2000-&

[9] CONFORMATIONS OF CYCLOBUTANE [J].

COTTON, FA ;

FRENZ, BA .

TETRAHEDRON, 1974, 30 (12) :1587-1594

[10]

DRORY WL, 1889, CHEM BER, V22, P2260