QUANTITATIVE-DETERMINATION OF LEAD DIOXIDE POLYMORPHS BY X-RAY-POWDER DIFFRACTOMETRY

被引：10

作者：

SKIDMORE, PR

SCHWARZ, RR

机构：

[1] Berec Group Limited, Group Technical Centre

来源：

ANALYST | 1979年 / 104卷 / 1243期

关键词：

Lanthanum hydroxide; Lead dioxide; Lead sulphate; Quantitative phase analysis; X-ray diffraction;

D O I：

10.1039/an9790400952

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The X-ray diffractometric methods used by previous workers to analyse positive plate material from lead-acid batteries for α-, β- and amorphous lead dioxides are critically appraised. In addition two alternative approaches, not previously applied to this problem, are assessed. An internal standard method is considered to be the best.

引用

页码：952 / 960

页数：9

共 18 条

[1] ELECTRODE POTENTIALS AND THERMAL DECOMPOSITION OF ALPHA- AND BETA-PBO2 [J].