ONE-DIMENSIONAL DOUBLE-QUANTUM MAGIC-ANGLE-SPINNING NMR OF DEUTERATED SOLIDS

被引：4

作者：

YANG, DW ^{[1
]}

YE, CH ^{[1
]}

机构：

[1] CHINESE ACAD SCI,WUHAN INST PHYS,MAGNET RESONANCE & ATOM & MOLEC PHYS LAB,WUHAN 430017,PEOPLES R CHINA

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1993年 / 2卷 / 04期

关键词：

RAMAN MAGNETIC RESONANCE; MAGIC-ANGLE SPINNING; MULTIPLE-QUANTUM NMR;

D O I：

10.1016/0926-2040(93)90020-N

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

An approach to double-quantum magic-angle spinning (2Q-MAS) of spin I = 1 with a time-share irradiation, resulting in a one-dimensional (1D) MQ spectrum, is demonstrated in this paper. The experiment was carried out with perdeuterated dimethoxybenzene and showed that the 2Q transitions were insensitive to the spinning axis deviation from the magic angle. The 1D-2Q-MAS scheme may also be applied to nitrogen-containing solids.

引用

页码：147 / 150

页数：4

共 10 条

[1] NUCLEAR RESONANCE SATURATION EFFECTS AND MULTIPLE-QUANTUM TRANSITIONS [J].