1,8-DEHYDRONAPHTHALENE .2. GENERATION OF 1,8-DEHYDRONAPHTHALENE FROM 1-AMINONAPHTHO[1,8-DE]TRIAZINE

被引：25

作者：

HOFFMANN, RW

GUHN, G

PREISS, M

DITTRICH, B

机构：

[1] Technische Hochschule, Darmstadt

来源：

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC | 1969年 / 05期

关键词：

D O I：

10.1039/j39690000769

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Amination of naphtho[1,8-de]triazine with hydroxylamine-O-sulphonate afforded 1-amino-8-azido-1-naphthalene and 1-aminonaphtho[1,8-de]triazine. Oxidation of the latter with lead tetra-acetate liberated nitrogen and gave 1,8-dehydronaphthalene which could be trapped by cycloaddition to dimethyl acetylenedicarboxylate or to N-phenylmaleimide.

引用

页码：769 / &

共 14 条

[1]

[Anonymous], ANGEW CHEM

[2]

CAMPBELL CD, 1964, P CHEM SOC LONDON, P296

[3] KONSTITUTION UND BILDUNG DER ARYLSULFONYL-DERIVATE VON AMINOHETEROCYCLEN [J].