SIMPLIFIED LIQUID-CHROMATOGRAPHIC DETERMINATION OF GLYPHOSATE AND METABOLITE RESIDUES IN ENVIRONMENTAL WATER USING POSTCOLUMN FLUOROGENIC LABELING

被引:23
作者
WIGFIELD, YY
LANOUETTE, M
机构
[1] Laboratory Services Division, Food Production and Inspection Branch, Agriculture Canada, Ottawa
关键词
D O I
10.1016/S0003-2670(00)83495-9
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Glyphosate and its metabolite aminomethylphosphonic acid in environmental water can be preconcentrated with an anion-exchange column, eluted with potassium citrate solution and determined directly by liquid chromatography with a post-column reactor and a fluorescence detector. The limit of detection and average recovery are 1 μg 1-1 and 89.3% for glyphosate and 0.4 μg l-1 and 86.3% for the metabolite. © 1990.
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页码:311 / 314
页数:4
相关论文
共 9 条
[1]  
[Anonymous], 1980, ANAL CHEM, V52, P2242
[2]   VALIDATION OF AN ANALYTICAL RESIDUE METHOD FOR ANALYSIS OF GLYPHOSATE AND METABOLITE - AN INTERLABORATORY STUDY [J].
COWELL, JE ;
KUNSTMAN, JL ;
NORD, PJ ;
STEINMETZ, JR ;
WILSON, GR .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1986, 34 (06) :955-960
[3]   SIMULTANEOUS ESTERIFICATION AND ACYLATION OF PESTICIDES FOR ANALYSIS BY GAS-CHROMATOGRAPHY .1. DERIVATIZATION OF GLYPHOSATE AND (AMINOMETHYL)PHOSPHONIC ACID WITH FLUORINATED ALCOHOLS-PERFLUORINATED ANHYDRIDES [J].
DEYRUP, CL ;
CHANG, SM ;
WEINTRAUB, RA ;
MOYE, HA .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1985, 33 (05) :944-947
[5]   A SIMPLIFIED HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC RESIDUE PROCEDURE FOR THE DETERMINATION OF GLYPHOSATE HERBICIDE AND (AMINOMETHYL)PHOSPHONIC ACID IN FRUITS AND VEGETABLES EMPLOYING POSTCOLUMN FLUOROGENIC LABELING [J].
MOYE, HA ;
MILES, CJ ;
SCHERER, SJ .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1983, 31 (01) :69-72
[6]   DETERMINATION OF THE HERBICIDE GLYPHOSATE AND ITS MAJOR METABOLITE AMINOMETHYLPHOSPHONIC ACID BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AFTER FLUORESCENCE LABELING [J].
ROSEBOOM, H ;
BERKHOFF, CJ .
ANALYTICA CHIMICA ACTA, 1982, 135 (02) :373-377
[7]  
Seiber J. N., 1984, J AGR FOOD CHEM, V32, P681
[8]   SEPARATION OF GLYPHOSATE AND POSSIBLE METABOLITES BY THIN-LAYER CHROMATOGRAPHY [J].
SPRANKLE, P ;
SANDBERG, CL ;
MEGGITT, WF ;
PENNER, D .
WEED SCIENCE, 1978, 26 (06) :673-674
[9]  
THOMPSON DG, 1989, J ASSOC OFF ANA CHEM, V72, P355