CONFIGURATIONAL CORRELATION OF PROTON AND FLUORINE CHEMICAL-SHIFTS OF AMIDES FROM PHCHFC02H AND L1CH(NH2)L2 AMINES

被引：6

作者：

HAMMAN, S

机构：

来源：

JOURNAL OF FLUORINE CHEMISTRY | 1990年 / 50卷 / 03期

关键词：

D O I：

10.1016/S0022-1139(00)84998-2

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Proton and fluorine chemical shifts of amides from PhCHFCO2H (used as a chiral derivatizing agent) and amines L1CH(NH2)L2 are correlated with configuration in order to assign configuration of chiral amines by F-19 NMR spectroscopy.

引用

页码：327 / 338

页数：12

共 18 条

[1] NUCLEAR MAGNETIC RESONANCE STUDY OF TRIFLUOROACETAMIDE AND N-METHYLTRIFLUOROACETAMIDE [J].

AKIYAMA, H ;

YAMAUCHI, F ;

OUCHI, K .

JOURNAL OF THE CHEMICAL SOCIETY B-PHYSICAL ORGANIC, 1971, (05) :1014-&

[2]

BARRELLE M, 1990, J CHEM RES-S, P100

[3]

BARRELLE M, 1990, J CHEM RES M, P701

[4] CYANOHYDRIDOBORATE ANION AS A SELECTIVE REDUCING AGENT [J].

BORCH, RF ;

BERNSTEIN, MD ;

DURST, HD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1971, 93 (12) :2897-+

[5]

BREUER W, 1982, J CHEM RES-S, P271

[6]

BREUER W, 1982, J CHEM RES M, P2901

[7] CONFORMATIONAL STUDIES OF PEPTIDE SYSTEMS - ROTATIONAL STATES OF NH-CH FRAGMENT OF ALANINE DIPEPTIDES BY NUCLEAR MAGNETIC RESONANCE [J].

BYSTROV, VF ;

PORTNOVA, SL ;

TSETLIN, VI ;

IVANOV, VT ;

OVCHINNIKOV, YA .

TETRAHEDRON, 1969, 25 (03) :493-+

[8] NUCLEAR MAGNETIC-RESONANCE ENANTIOMER REAGENTS - CONFIGURATIONAL CORRELATIONS VIA NUCLEAR MAGNETIC-RESONANCE CHEMICAL-SHIFTS OF DIASTEREOMERIC MANDELATE, O-METHYLMANDELATE, AND ALPHA-METHOXY-ALPHA-TRIFLUOROMETHYLPHENYLACETATE (MTPA) ESTERS [J].

DALE, JA ;

MOSHER, HS .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1973, 95 (02) :512-519

[9] DIRECTED RESOLUTION OF 2-FLUORO-2-METHYLHEXANOIC ACID [J].

DEMUNARI, S ;

MARAZZI, G ;

FAUSTINI, F ;

VILLA, V ;

CARLUCCIO, L .

JOURNAL OF FLUORINE CHEMISTRY, 1986, 34 (01) :157-166

[10] 2-FLUORO-2-PHENYL ACETIC-ACID - SYNTHESIS, ABSOLUTE-CONFIGURATION AND USE AS A DERIVATIZING CHIRAL AGENT [J].

HAMMAN, S ;

BARRELLE, M ;

TETAZ, F ;

BEGUIN, CG .

JOURNAL OF FLUORINE CHEMISTRY, 1987, 37 (01) :85-94

← 1 2 →