Recently, chemical process operations are becoming more precise, making process control more difficult by conventional dynamics and control theories alone. The zone melting process considered in this work is a typical example of advanced chemical processes and requires highly precise operations. A precise temperature profile must be achieved and maintained against strong disturbances due to the movement of a sample tube or heaters and to interactions between heaters. To overcome this difficult problem, a new zone melting process is proposed in this paper. Without movement of either sample tube or heaters, realization of, the desired time-varying temperature profile is attempted by manipulation of fixed heaters. The process dynamics are treated as a distributed-parameter system. Applying distributed parameter control to the zone melting process in a simulation, stimulation verified that the process could be realized. Moreover, experimental results using an anthracene zone melting apparatus also showed good control performance.