METHOD FOR RADIOCAPILLARY GAS-CHROMATOGRAPHY EMPLOYING A MODIFIED OXIDATION REDUCTION TRAIN AND FLOW-THROUGH DETECTOR

被引:16
作者
CROTEAU, RB
SATTERWHITE, DM
机构
[1] Institute of Biological Chemistry, Washington State University, Pullman
来源
JOURNAL OF CHROMATOGRAPHY | 1990年 / 500卷
关键词
D O I
10.1016/S0021-9673(00)96076-X
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A conventional radioactivity monitor was modified by reducing the volume of the oxidation-reduction train and gas proportional counting tube to permit coupled radio-capillary gas chromatographic analysis of labeled isomeric metabolites. The utility of this radioactivity monitoring technique was demonstrated by separating 3H-labeled sesquiterpene olefins. The advantages and limitations of mass (thermal conductivity) and radioactivity detection by this method are discussed. © 1990.
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页码:349 / 354
页数:6
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