SOLVENT SYSTEM SELECTION FOR SEPARATION OF ANTHRAQUINONES BY MEANS OF CENTRIFUGAL PARTITION CHROMATOGRAPHY - APPLICATION TO AN EXTRACT OF A RUBIA-TINCTORUM HAIRY ROOT CULTURE

被引：6

作者：

HERMANSLOKKERBOL, ACJ

VANDERHEIJDEN, R

VERPOORTE, R

机构：

[1] Division of Pharmacognosy, Center for Bio-Pharmaceutical Sciences, Gorlaeus Laboratories, Leiden University, 2300, RA Leiden

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY | 1993年 / 16卷 / 07期

关键词：

D O I：

10.1080/10826079308020963

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Two two-phase systems were selected for the separation of anthraquinones by means of centrifugal partition chromatography, using alizarin, purpurin and quinizarin as test substances. These systems were applied to the separation of anthraquinones, extracted from a Rubia tinctorum hairy root culture. Some of the anthraquinones present were identified: alizarin, alizarin 1-methyl ether, lucidin and nordamnacanthal.

引用

页码：1433 / 1451

页数：19

共 16 条

[1] CENTRIFUGAL PARTITION CHROMATOGRAPHY .4. PREPARATIVE SAMPLE PURIFICATION AND PARTITION-COEFFICIENT DETERMINATION [J].

BERTHOD, A ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (06) :1187-1204

[2] CENTRIFUGAL PARTITION CHROMATOGRAPHY .6. TEMPERATURE EFFECTS [J].

BERTHOD, A ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (07) :1457-1474

[3] CENTRIFUGAL PARTITION CHROMATOGRAPHY .2. SELECTIVITY AND EFFICIENCY [J].

BERTHOD, A ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (03) :567-583

[4] CENTRIFUGAL PARTITION CHROMATOGRAPHY .1. GENERAL FEATURES [J].

BERTHOD, A ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (03) :547-566

[5] CENTRIFUGAL PARTITION CHROMATOGRAPHY .5. OCTANOL-WATER PARTITION-COEFFICIENTS, DIRECT AND INDIRECT DETERMINATION [J].

BERTHOD, A ;

HAN, YI ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (07) :1441-1456

[6] CENTRIFUGAL PARTITION CHROMATOGRAPHY .3. PHYSICOCHEMICAL PROPERTIES OF TERNARY LIQUID-SYSTEMS [J].

BERTHOD, A ;

DUNCAN, JD ;

ARMSTRONG, DW .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (06) :1171-1185

[7] STUDY OF ACOH-HCOOH-H2O-CHCL3 SOLVENT SYSTEM APPLICATION TO THE SEPARATION OF 2 LARGE AND HYDROPHOBIC FRAGMENTS OF BACTERIORHODOPSIN MEMBRANE-PROTEIN BY CENTRIFUGAL PARTITION CHROMATOGRAPHY [J].

FOUCAULT, A ;

NAKANISHI, K .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1988, 11 (12) :2455-2472

[8] LIQUID LIQUID PARTITION CHROMATOGRAPHY IN NATURAL PRODUCT ISOLATION [J].

HOSTETTMANN, K ;

MARSTON, A .

ANALYTICA CHIMICA ACTA, 1990, 236 (01) :63-76

[9] QUINONES AND RELATED-COMPOUNDS IN HIGHER-PLANTS .12. ANTHRAQUINONES IN CELL-SUSPENSION CULTURES OF MORINDA-CITRIFOLIA [J].

INOUE, K ;

NAYESHIRO, H ;

INOUYE, H ;

ZENK, M .

PHYTOCHEMISTRY, 1981, 20 (07) :1693-1700

[10]

KOBLITZ H, 1988, CELL CULTURE SOMATIC, V5, P113

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