SYNTHESIS AND X-RAY STRUCTURE DETERMINATION OF THE MIXED ALKALI-METAL ORTHONITRATE NA3K3(NO4)2

被引：3

作者：

BREMM, T ^{[1
]}

JANSEN, M ^{[1
]}

机构：

[1] UNIV BONN,INST ANORGAN CHEM,GERHARD DOMAGK STR 1,W-5300 BONN 1,GERMANY

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 1991年 / 46卷 / 08期

关键词：

ALKALI METAL ORTHONITRATES; SYNTHESIS; CRYSTAL STRUCTURE; RAMAN SPECTRA; IR SPECTRA;

D O I：

10.1515/znb-1991-0810

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The title compound has been characterized by X-ray powder and single crystal diffraction: Pbcn; a = 7.2961(1), b = 15.997(4), c = 7.016(1) angstrom; Z = 4; 1514 diffractometer data, R = 0.04, R(w) = 0.03. The vibrational spectra are compatible with a tetrahedral geometry of the anion.

引用

页码：1031 / 1034

页数：4

共 9 条

[1]

BRAUER G, 1978, HDB PRAPARATIVEN ANO, V2, P953

[2]

BREMM T, UNPUB

[3]

Hahn, 1983, INT TABLES CRYSTALLO

[4]

JANSEN M, 1982, Z ANORG ALLG CHEM, V491, P175, DOI 10.1002/zaac.19824910122

[5]

KLEMENC A, 1951, Z ANORG ALLG CHEM, V265, P221

[6] DETERMINATION OF CRYSTAL-STRUCTURE OF T-NA3PO4 WITH X-RAY AND NEUTRON POWER DIFFRACTION [J].

LISSEL, E ;

JANSEN, M ;

JANSEN, E ;

WILL, G .

ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1990, 192 (3-4) :233-243

[7] PARST - A SYSTEM OF FORTRAN ROUTINES FOR CALCULATING MOLECULAR-STRUCTURE PARAMETERS FROM RESULTS OF CRYSTAL-STRUCTURE ANALYSES [J].

NARDELLI, M .

COMPUTERS & CHEMISTRY, 1983, 7 (03) :95-98

[8]

SHELDRICK GM, 1976, SHELXS 86 SHELX 76 P

[9] ON NA3PO4 - PREPARATIVE INVESTIGATIONS, CRYSTAL-STRUCTURE OF HIGH-TEMPERATURE FORM [J].

WIENCH, DM ;

JANSEN, M .

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1980, 461 (02) :101-108

← 1 →