BENZYLTRIETHYLAMMONIUM TETRATHIOMOLYBDATE - AN IMPROVED SULFUR TRANSFER REAGENT FOR THE SYNTHESIS OF DISULFIDES

被引：58

作者：

RAMESHA, AR ^{[1
]}

CHANDRASEKARAN, S ^{[1
]}

机构：

[1] INDIAN INST SCI,DEPT ORGAN CHEM,BANGALORE 560012,KARNATAKA,INDIA

来源：

SYNTHETIC COMMUNICATIONS | 1992年 / 22卷 / 22期

关键词：

D O I：

10.1080/00397919208021143

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Benzyltriethylammonium tetrathiomolybdate has been found to be a superior reagent for the conversion of alkyl halides to the corresponding disulfides in chloroform at room temperature.

引用

页码：3277 / 3284

页数：8

共 17 条

[1]

CARALLO AS, 1967, B SOC CHIM FR, V2, P517

[2]

COHEN VI, 1976, HELV CHIM ACTA, V59, P840

[3] CHEMISTRY OF TETRATHIOTUNGSTATES - A NOVEL SYNTHESIS OF DISULFIDES FROM SULFONYL DERIVATIVES [J].

DHAR, P ;

RANJAN, R ;

CHANDRASEKARAN, S .

JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (12) :3728-3729

[4]

DHAR P, 1992, S J ORG CHEM, V57, P1699

[5]

DHAR P, 1989, S J ORG CHEM, V54, P2989

[6] ORGANIC DISULFIDES AND RELATED SUBSTANCES .1. OXIDATION OF THIOLS TO DISULFIDES WITH LEAD TETRAACETATE [J].

FIELD, L ;

LAWSON, JE .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1958, 80 (04) :838-841

[7] ORGANOTIN-MEDIATED SELECTIVE DESULFURIZATION - TRI-NORMAL-BUTYLTIN HYDRIDE REDUCTION OF UNSYMMETRIC SULFIDES [J].

GUTIERREZ, CG ;

SUMMERHAYS, LR .

JOURNAL OF ORGANIC CHEMISTRY, 1984, 49 (26) :5206-5213

[8] NOVEL ALKYNE REACTIONS WITH BINUCLEAR MOLYBDENUM-SULFUR COMPLEXES - STRUCTURE OF THE DIMETHYL ACETYLENEDICARBOXYLATE ADDUCT OF [MO2O2(MU-S)2(S2)2]2- [J].

HALBERT, TR ;

PAN, WH ;

STIEFEL, EI .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1983, 105 (16) :5476-5477

[9]

HISKEY RG, 1968, J ORG CHEM, V32, P563

[10]

LUCAS CR, 1970, CAN J CHEM, V48, P1869

← 1 2 →