REACTIONS OF A CYCLOTRISILANE WITH ALKYNES - SYNTHESIS AND FIRST CRYSTAL-STRUCTURE OF 1,2-DISILACYCLOBUT-3-ENES

被引：24

作者：

BELZNER, J ^{[1
]}

IHMELS, H ^{[1
]}

KNEISEL, BO ^{[1
]}

HERBSTIRMER, R ^{[1
]}

机构：

[1] UNIV GOTTINGEN,INST ANORGAN CHEM,D-37077 GOTTINGEN,GERMANY

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1994年 / 17期

关键词：

D O I：

10.1039/c39940001989

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

1,2-Disilacyclobut-3-enes are synthesized quantitatively from cyclotrisilane 1 and alkynes; the solid-state structure of 4d is determined by single-crystal X-ray diffraction.

引用

页码：1989 / 1990

页数：2

共 21 条

[1] PHOTOINDUCED ELECTRON-TRANSFER OXYGENATION OF 1,2-DISILETENE
AKASAKA, T
SATO, K
KAKO, M
ANDO, W
[J]. TETRAHEDRON, 1992, 48 (16) : 3283 - 3292
[2] PREPARATION OF "HEXAMETHYL-1,2-DISILA-3-CYCLOBUTENE
ATWELL, WH
UHLMANN, JG
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1973, 52 (02) : C21 - C23
[3] ALTERNATIVE MECHANISM FOR FORMATION OF 1,4-DISILACYCLOHEXA-2,5-DIENES FROM ACETYLENES AND SILYLENES
BARTON, TJ
KILGOUR, JA
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1976, 98 (24) : 7746 - 7751
[4] BARTON TJ, 1982, COMPREHENSIVE ORGANO, P206
[5] A NOVEL ROUTE TO STABLE SILACYCLOPROPENES - 1ST SYNTHESIS OF SILACYCLOPROPENES BEARING VINYLIC HYDROGEN
BELZNER, J
IHMELS, H
[J]. TETRAHEDRON LETTERS, 1993, 34 (41) : 6541 - 6544
[6] DEYOUNG DJ, 1987, MAIN GROUP MET CHEM, V1, P19
[7] THE MOLECULAR STRUCTURE OF CYCLOBUTENE, C4H6
GOLDISH, E
HEDBERG, K
SCHOMAKER, V
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1956, 78 (12) : 2714 - 2716
[8] SYNTHESIS AND REACTIONS OF POLYSILACYCLOALKYNES
HOJO, F
SEKIGAWA, S
NAKAYAMA, N
SHIMIZU, T
ANDO, W
[J]. ORGANOMETALLICS, 1993, 12 (03) : 803 - 810
[9] SYNTHESIS AND STRUCTURE OF DIGERMACYCLOBUTENES AND DISTANNACYCLOBUTENES
KREBS, A
JACOBSENBAUER, A
HAUPT, E
VEITH, M
HUCH, V
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1989, 28 (05): : 603 - 604
[10] KREBS A, 1989, ANGEW CHEM, V101, P640

← 1 2 3 →