INFLUENCE OF STORAGE-CONDITIONS ON ALUMINUM CONCENTRATIONS IN SERUM, DIALYSIS FLUID, URINE, AND TAP WATER

被引:21
作者
WILHELM, M
OHNESORGE, FK
机构
[1] Institute of Toxicology, Heinrich-Heine University of Diüsseldorf, Diüsseldorf 1, D.4000
关键词
D O I
10.1093/jat/14.4.206
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The Influence of storage temperature, vessel type, and treatment on alterations of aluminum (AI) concentrations in serum, urine, and dialysis fluid samples was studied at three different concentrations for each sample over an 18-month period. Furthermore, the influence of acidification on AI levels in tap water, urine, and dialysis fluid samples was studied over a four-month period. AI was measured by atomic absorption spectrometry. Sample storage in glass vessels was unsuitable, whereas only minor alterations of AI levels were observed with storage in polypropylene tubes, polystyrene tubes, and Monovettes. By using appropriate plastic containers, acid washing of the vessels showed no improvement. Frozen storage was superior compared with 4°C whereas storage at 80°C offered no advantage compared with storage at 20°C. Acidification of tap water samples was necessary to stabilize AI levels during storage. No striking effect of acidification on AI levels in urine and dialysis fluid samples was found. It is concluded that long-term storage of serum, urine, tap water, and dialysis fluid samples is possible if appropriate conditions are used. © 1990 Oxford University Press.
引用
收藏
页码:206 / 210
页数:5
相关论文
共 19 条
[1]  
ANDERSEN JR, 1986, ANALYST, V11, P657
[2]   SERUM ALUMINUM CANNOT BE MEASURED ACCURATELY [J].
BERLYNE, GM ;
ADLER, AJ .
AMERICAN JOURNAL OF KIDNEY DISEASES, 1985, 6 (05) :288-292
[3]  
BERTHOLF RL, 1983, CLIN CHEM, V29, P1087
[4]  
BERTRAM HP, 1981, NIEREN HOCHDRUCK, V10, P188
[5]  
BROWN S, 1984, CLIN CHEM, V30, P1216
[6]   DETERMINATION OF ALUMINUM IN BODY-FLUIDS BY SOLVENT-EXTRACTION AND ATOMIC-ABSORPTION SPECTROSCOPY WITH ELECTROTHERMAL ATOMIZATION [J].
BURATTI, M ;
CARAVELLI, G ;
CALZAFERRI, G ;
COLOMBI, A .
CLINICA CHIMICA ACTA, 1984, 141 (2-3) :253-259
[7]  
Cornelis R, 1984, Contrib Nephrol, V38, P1
[8]  
GUILLARD O, 1988, CLIN CHEM, V34, P1603
[9]   IMPROVED DETERMINATION OF ALUMINUM IN SERUM BY ELECTROTHERMAL ATOMIC-ABSORPTION SPECTROMETRY AND ZEEMAN BACKGROUND CORRECTION [J].
GUILLARD, O ;
TIPHANEAU, K ;
REISS, D ;
PIRIOU, A .
ANALYTICAL LETTERS PART B-CLINICAL AND BIOCHEMICAL ANALYSIS, 1984, 17 (14) :1593-1605
[10]  
LEUNG FY, 1983, CLIN CHEM, V29, P1966