SYNTHESIS AND NUCLEAR-MAGNETIC-RESONANCE STUDIES OF SOME L-FUCOSYL-CONTAINING DISACCHARIDES

被引：16

作者：

BAUMANN, H

JANSSON, PE

KENNE, L

机构：

[1] Department of Organic Chemistry, Arrhenius Laboratory, Stockholm University

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 | 1991年 / 09期

关键词：

D O I：

10.1039/p19910002229

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Eleven disaccharides containing an L-fucosyl group have been synthesized and their H-1 and C-13 NMR spectra assigned. HSEA analysis has indicated which inter-residue atomic interactions are present in the disaccharides, some of which could be correlated with observed glycosylation shifts. The results give further knowledge about glycosylation shifts, valuable for the interpretation of NMR spectra of larger saccharides.

引用

收藏

页码：2229 / 2233

页数：5

相关论文

共 16 条

[1] NMR AND CONFORMATIONAL STUDIES ON SOME 1,3-LINKED DISACCHARIDES [J].

BAUMANN, H ;

JANSSON, PE ;

KENNE, L .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1988, (02) :209-217

[2] CALCIUM CARBOHYDRATE BRIDGES COMPOSED OF UNCHARGED SUGARS - STRUCTURE OF A HYDRATED CALCIUM BROMIDE COMPLEX OF ALPHA-FUCOSE [J].

COOK, WJ ;

BUGG, CE .

BIOCHIMICA ET BIOPHYSICA ACTA, 1975, 389 (03) :428-435

[3] REDUCTIVE RING OPENINGS OF CARBOHYDRATE BENZYLIDENE ACETALS USING BORANE-TRIMETHYLAMINE AND ALUMINUM-CHLORIDE - REGIOSELECTIVITY AND SOLVENT DEPENDENCE [J].

EK, M ;

GAREGG, PJ ;

HULTBERG, H ;

OSCARSON, S .

JOURNAL OF CARBOHYDRATE CHEMISTRY, 1983, 2 (03) :305-311

[4] THIOGLYCOSIDES AS GLYCOSYLATING AGENTS IN OLIGOSACCHARIDE SYNTHESIS [J].

FUGEDI, P ;

GAREGG, PJ ;

LONN, H ;

NORBERG, T .

GLYCOCONJUGATE JOURNAL, 1987, 4 (02) :97-108

[5] MONOBENZYLATION OF DIOLS USING PHASE-TRANSFER CATALYSIS [J].

GAREGG, PJ ;

IVERSEN, T ;

OSCARSON, S .

CARBOHYDRATE RESEARCH, 1976, 50 (02) :C12-C14

[6] COMPUTER-ASSISTED STRUCTURAL-ANALYSIS OF POLYSACCHARIDES WITH AN EXTENDED VERSION OF CASPER USING H-1-NMR AND C-13-NMR DATA [J].

JANSSON, PE ;

KENNE, L ;

WIDMALM, G .

CARBOHYDRATE RESEARCH, 1989, 188 :169-191

[7] SYNTHESIS OF AND NUCLEAR-MAGNETIC-RESONANCE AND CONFORMATIONAL STUDIES ON SOME 1,2-LINKED DISACCHARIDE METHYL GLYCOSIDES CONTAINING D-MANNOSE AND L-RHAMNOSE [J].

JANSSON, PE ;

KENNE, L ;

OTTOSSON, H .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1990, (07) :2011-2018

[8]

JEFFREY GA, 1977, ACTA CRYSTALLOGR B, V33, P428

[9]

KOLARE I, UNPUB

[10] THE CONFORMATIONS OF OLIGOSACCHARIDES RELATED TO THE ABH AND LEWIS HUMAN-BLOOD GROUP DETERMINANTS [J].

LEMIEUX, RU ;

BOCK, K ;

DELBAERE, LTJ ;

KOTO, S ;

RAO, VS .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1980, 58 (06) :631-653