1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .46. C-13 NMR-SPECTRA OF 8-ARYL-8-AZABICYCLO[3.2.1]OCT-3-EN-2-ONES AND RELATED COMPOUNDS

被引：10

作者：

KATRITZKY, AR

DENNIS, N

SABONGI, GJ

机构：

[1] School of Chemical Sciences, University of East Anglia, Norwich

来源：

ORGANIC MAGNETIC RESONANCE | 1979年 / 12卷 / 06期

关键词：

D O I：

10.1002/mrc.1270120606

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Carbon‐13 NMR spectra of various 8‐aryl‐8‐azabicyclo[3.2.1]oct‐3‐en‐2‐ones and other related compounds, including tropinone, were determined, and the predominant conformation at the bridgehead nitrogen was established. The full assignment of resonances from proton decoupled and coupled spectra was based on the analysis of the splitting pattern and characteristic chemical shifts. The use of the determined 13C NMR spectra in the assignment of 13C NMR data in related but more complicated structures is also proposed. Copyright © 1979 Heyden & Son Ltd.

引用

页码：357 / 361

页数：5

共 14 条

[1]

BREITMAIER E, 1974, MONOGRAPHS MODERN CH, V5, P154

[2] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .18. ADDUCTS FROM 3-OXIDO-1-PHENYLPYRIDINIUM AND THEIR QUATERNIZATION AND CONVERSION INTO TROPONE DERIVATIVES [J].

DENNIS, N ;

KATRITZKY, AR ;

PARTON, SK ;

NOMURA, Y ;

TAKAHASHI, Y ;

TAKEUCHI, Y .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1976, (21) :2289-2296

[3] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .20. PREPARATION AND DIMERIZATION OF 1-(5-NITRO-2-PYRIDYL) AND 1-(4,6-DIMETHYLPYRIMIDIN-2-YL) 3-OXIDOPYRIDINIUM [J].

DENNIS, N ;

IBRAHIM, B ;

KATRITZKY, AR .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1976, (21) :2296-2307

[4] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .17. SYNTHETIC APPLICATIONS OF HETEROAROMATIC BETAINES WITH 6-MEMBERED RINGS [J].

DENNIS, N ;

KATRITZKY, AR ;

TAKEUCHI, Y .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1976, 15 (01) :1-9

[5] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .11. THERMAL CYCLOADDITIONS OF 1-(5-NITRO-2-PYRIDYL) AND 1-(4,6-DIMETHYLPYRIMIDIN-2-YL) 3-OXIDOPYRIDINIUM WITH 2, 4, AND 6 PI-ELECTRON COMPONENTS [J].

DENNIS, N ;

IBRAHIM, B ;

KATRITZKY, AR .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1976, (21) :2307-2328

[6] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .33. TRANSFORMATIONS OF CYCLOADDUCTS DERIVED FROM 3-OXIDO-1-TRIAZINYLPYRIDINIUMS [J].

DENNIS, N ;

KATRITZKY, AR ;

SABOUNJI, GJ ;

TURKER, L .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1977, (17) :1930-1940

[7] 1,3-DIPOLAR CHARACTER OF 6-MEMBERED AROMATIC RINGS .9. REARRANGEMENT AND ADDITIONS OF 1-(2,4-DINITROPHENYL)-3-OXIDOPYRIDINIUM [J].

DENNIS, N ;

IBRAHIM, B ;

KATRITZK.AR ;

TAULOV, IG ;

TAKEUCHI, Y .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1974, (15) :1883-1887

[8]

IBRAHIM B, 1975, THESIS E ANGLIA, P220

[9]

KATRITZKY AR, UNPUBLISHED

[10]

Lippmaa E., 1970, ORG MAGN RESON, V2, P581, DOI DOI 10.1002/MRC.1270020609

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