IRIDIUM OXIDE PH MICROELECTRODE

被引:56
作者
VANHOUDT, P
LEWANDOWSKI, Z
LITTLE, B
机构
[1] MONTANA STATE UNIV,NATL SCI FDN,INTERFACIAL MICROBIAL PROC ENGN RES CTR,BOZEMAN,MT 59717
[2] NAVAL RES LAB DETACHMENT,STENNIS SPACE CTR,BAY ST LOUIS,MS 39529
关键词
PH MEASUREMENT; MICROELECTRODES; MICROENVIRONMENTS; BIOFILMS;
D O I
10.1002/bit.260400507
中图分类号
Q81 [生物工程学(生物技术)]; Q93 [微生物学];
学科分类号
071005 ; 0836 ; 090102 ; 100705 ;
摘要
The manufacture, calibration, and signal conditioning during construction of an iridium/iridium oxide pH microsensor is described. The microsensor was designed to be used extracellularly, primarily in biofilm research. The sensing tip diameters were typically in the range of 3-15-mu-m. The iridium oxide was formed by potential cycling in dilute sulfuric acid. A pH profile across a denitrifying biofilm was measured as an example of an application. The higher Nernstian slope (70-80 mV/pH for fresh electrodes), increased rigidity, and restriction of the sensing tip to the outermost end of the electrode are features which make the iridium/iridium oxide pH microelectrode superior to a glass microelectrode.
引用
收藏
页码:601 / 608
页数:8
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