ANALYSIS OF COUMARINS BY MICRO-HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY WITH A PARTICLE-BEAM INTERFACE

被引：26

作者：

CAPPIELLO, A ^{[1
]}

FAMIGLINI, G ^{[1
]}

MANGANI, F ^{[1
]}

TIRILLINI, B ^{[1
]}

机构：

[1] UNIV URBINO,IST BOT & ORTO BOT,I-61029 URBINO,ITALY

来源：

JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY | 1995年 / 6卷 / 02期

关键词：

D O I：

10.1016/S1044-0305(94)00096-I

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Coumarins are a large group of compounds that are naturally present in plant tissues and that exhibit a wide range of pharmacological properties. Analytical methods based on chromatographic techniques and conventional detectors are inadequate to accurately analyze coumarins in complex matrices such as plant extracts. In this article a new method based on a modified particle beam liquid chromatography-mass spectrometry interface is described. The method allows specific and accurate determination of several coumarins in biological matrices. An application regarding the analysis of 18 coumarins in the extract of Smyrnium perfoliatum L. is also reported.

引用

页码：132 / 139

页数：8

共 35 条

[1] LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY USING GLASS LINED STAINLESS-STEEL MICROBORE COLUMNS
ALCOCK, NJ
CORBELLI, L
GAMES, DE
LANT, MS
WESTWOOD, SA
[J]. BIOMEDICAL MASS SPECTROMETRY, 1982, 9 (11): : 499 - 504
[2] LIQUID-CHROMATOGRAPHY - PARTICLE-BEAM MASS-SPECTROMETRY FOR IDENTIFICATION OF UNKNOWN POLLUTANTS IN WATER
BAGHERI, H
SLOBODNIK, J
RECASENS, RMM
GHIJSEN, RT
BRINKMAN, UAT
[J]. CHROMATOGRAPHIA, 1993, 37 (3-4) : 159 - 167
[3] LIQUID-CHROMATOGRAPHY PARTICLE BEAM MASS-SPECTROMETRY OF POLAR COMPOUNDS OF ENVIRONMENTAL INTEREST
BEHYMER, TD
BELLAR, TA
BUDDE, WL
[J]. ANALYTICAL CHEMISTRY, 1990, 62 (15) : 1686 - 1690
[4] BERLONI A, UNPUB CHROMATOGRAPHI
[5] A COMPARISON OF ELECTRON-IMPACT MASS-SPECTROMETRY OF ISOMERIC PYRANOCOUMARINS "(PYRANO[3,2-C][1]BENZOPYRAN-5-ONES) AND PYRANOCHROMONES "(PYRANO[2,3-B][1]BENZOPYRAN-5-ONES)
BRAVO, P
TICOZZI, C
DAOLIO, S
TRALDI, P
[J]. ORGANIC MASS SPECTROMETRY, 1985, 20 (12): : 740 - 747
[6] STANDARDIZATION OF TEST CONDITIONS FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY COLUMNS
BRISTOW, PA
KNOX, JH
[J]. CHROMATOGRAPHIA, 1977, 10 (06) : 279 - 289
[7] NEW MATERIALS AND PACKING TECHNIQUES FOR MICRO-HPLC PACKED CAPILLARY COLUMNS
CAPPIELLO, A
PALMA, P
MANGANI, F
[J]. CHROMATOGRAPHIA, 1991, 32 (7-8) : 389 - 391
[8] EVALUATION OR THE PERFORMANCE OF A MICROFLOW RATE LC/MS PARTICLE-BEAM INTERFACE
CAPPIELLO, A
FAMIGLINI, G
[J]. ANALYTICAL CHEMISTRY, 1994, 66 (22) : 3970 - 3976
[9] MICRO FLOW-RATE PARTICLE BEAM INTERFACE FOR CAPILLARY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY
CAPPIELLO, A
BRUNER, F
[J]. ANALYTICAL CHEMISTRY, 1993, 65 (09) : 1281 - 1287
[10] DETERMINATION OF ACIDIC AND BASIC NEUTRAL PESTICIDES IN WATER WITH A NEW MICROLITER FLOW-RATE LC/MS PARTICLE-BEAM INTERFACE
CAPPIELLO, A
FAMIGLINI, G
BRUNER, F
[J]. ANALYTICAL CHEMISTRY, 1994, 66 (09) : 1416 - 1423

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