ACQUISITION OF POWDER DIFFRACTION DATA WITH SYNCHROTRON RADIATION

被引:89
作者
COX, DE
TOBY, BH
EDDY, MM
机构
[1] UNIV CALIF SANTA BARBARA,DEPT CHEM,SANTA BARBARA,CA 93106
[2] UNION CARBIDE CORP,CENT SCI LAB,TARRYTOWN,NY 10951
来源
AUSTRALIAN JOURNAL OF PHYSICS | 1988年 / 41卷 / 02期
关键词
Accelerators; Synchrotron--Applications; -; Crystals--Structure; Diffractometers; X-Rays--Diffraction;
D O I
10.1071/PH880117
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
During the past year, a dedicated triple-axis powder diffractometer has been in routine operation at the Brookhaven National Synchrotron Light Source as a user-oriented facility. The diffractometer is designed to allow easy interchange between energy-dispersive and monochromatic beam experiments. In the latter mode of operation, high resolution data have been collected for a variety of samples with the use of the crystal-analyzer technique, and in several cases these data sets have been used successfully for structure solution and Rietveld refinement. Several aspects of data acquisition at a synchrotron beam-line are described, and some of the different types of scattering geometry which have been used are discussed.
引用
收藏
页码:117 / 131
页数:15
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