MAGNETIC-PROPERTIES OF ULTRAFINE FE-NI-B PARTICLES

被引:20
作者
NAFIS, S [1 ]
HADJIPANAYIS, GC [1 ]
SORENSEN, CM [1 ]
KLABUNDE, KJ [1 ]
机构
[1] KANSAS STATE UNIV AGR & APPL SCI,DEPT CHEM,MANHATTAN,KS 66506
关键词
D O I
10.1063/1.344887
中图分类号
O59 [应用物理学];
学科分类号
摘要
Ultrafine Fe-Ni-B particles were synthesized by reducing iron and nickel salts with NaBH4 in aqueous solutions. The particles had diameters in the range of 100-300 Å. X-ray diffraction patterns showed that particles with boron concentration 18 at. % or more were amorphous; otherwise they were crystalline. It was also found that the amorphous particles contain less than 50 at. % of Fe. The coercivity of Fe-B particles was increased by an addition of a small amount of Ni to the system. The room-temperature coercivity and saturation magnetization for particles of composition Fe63Ni 24B13 and of diameter 100 Å were 1275 Oe and 70 emu/g, respectively.
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页码:4478 / 4480
页数:3
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