A DIGITAL PHASE-SHIFTER FOR MULTIPLE PULSE NMR

被引:7
作者
GERSTEIN, BC [1 ]
HAN, JW [1 ]
HWANG, SJ [1 ]
PAN, HJ [1 ]
SKANK, H [1 ]
机构
[1] IOWA STATE UNIV SCI & TECHNOL,DEPT CHEM,AMES,IA 50011
关键词
D O I
10.1063/1.1141362
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An eight bit digital phase shifter is described which is suitable for multiple pulse NMR of solids in terms of settling time (≅2 μs) and phase resolution (1.406°). The unit incorporates an 8-bit Merrimac digital phase shifter model PSDW-84-1, and an amplification-damping-pulse shaping circuit to solve the problem of variable attenuation as a function of phase setting. Results of multiple quantum spin counting and homonuclear dipolar decoupling experiments on ensembles of strongly dipolar coupled spin 1/2 systems are used to demonstrate the capability of the unit.
引用
收藏
页码:2349 / 2353
页数:5
相关论文
共 17 条
[1]  
[Anonymous], 1971, PULSE FOURIER TRANSF
[2]   ANALYSIS OF MULTIPLE PULSE NMR IN SOLIDS .3. [J].
BURUM, DP ;
RHIM, WK .
JOURNAL OF CHEMICAL PHYSICS, 1979, 71 (02) :944-956
[3]   SOLID-STATE NMR-STUDIES OF CADMIUM - CD-113-H-1 CROSS POLARIZATION AND MAGIC-ANGLE SPINNING [J].
CHEUNG, TTP ;
WORTHINGTON, LE ;
MURPHY, PD ;
GERSTEIN, BC .
JOURNAL OF MAGNETIC RESONANCE, 1980, 41 (01) :158-168
[4]  
Ernst R. R., 1987, PRINCIPLES MAGNETIC
[5]  
Gerstein B.C., 1985, TRANSIENT TECHNIQUES
[6]  
Haeberlen U., 1976, HIGH RESOLUTION NMR
[7]   TRANSIENT NUTATIONS AND SPIN ECHOES ASSOCIATED WITH 2-QUANTUM TRANSITION IN MULTILEVEL NMR SYSTEM [J].
HATANAKA, H ;
HASHI, T .
JOURNAL OF THE PHYSICAL SOCIETY OF JAPAN, 1975, 39 (04) :1139-1140
[8]   EXCITATION AND DETECTION OF COHERENCE BETWEEN FORBIDDEN LEVELS IN 3-LEVEL SPIN SYSTEM BY MULTISTEP PROCESSES [J].
HATANAKA, H ;
TERAO, T ;
HASHI, T .
JOURNAL OF THE PHYSICAL SOCIETY OF JAPAN, 1975, 39 (03) :835-836
[9]  
MEHRING M, 1981, HIGH RESOLUTION NMR
[10]  
Munowitz M, 1988, COHERENCE NMR