MATRIX-ASSISTED LASER-DESORPTION IONIZATION MASS-SPECTROMETRY OF POLYSACCHARIDES

被引：58

作者：

GARROZZO, D ^{[1
]}

IMPALLOMENI, G ^{[1
]}

SPINA, E ^{[1
]}

STURIALE, L ^{[1
]}

ZANETTI, F ^{[1
]}

机构：

[1] POLY TECH,AREA RIC,I-34012 TRIESTE,ITALY

来源：

RAPID COMMUNICATIONS IN MASS SPECTROMETRY | 1995年 / 9卷 / 10期

关键词：

D O I：

10.1002/rcm.1290091014

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

In this paper we report matrix-assisted laser desorption/ionization (MALDI) mass spectra of dextrans up to 100 000 Da molecular weight and compare these measurements with those obtained by conventional size-exclusion chromatography with low-angle laser light scattering (SEC/LALLS). These results extend the usefulness of MALDI-MS to higher molecular weight polysaccharides and give some insights into the MALDI process.

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页码：937 / 941

页数：5

相关论文

共 18 条

[1] QUANTITATIVE APPLICATIONS OF MATRIX-ASSISTED LASER-DESORPTION IONIZATION WITH TIME-OF-FLIGHT MASS-SPECTROMETRY - DETERMINATION OF COPOLYMER COMPOSITION IN BACTERIAL COPOLYESTERS [J].

ABATE, R ;

BALLISTRERI, A ;

MONTAUDO, G ;

GAROZZO, D ;

IMPALLOMENI, G ;

CRITCHLEY, G ;

TANAKA, K .

RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1993, 7 (11) :1033-1036

[2] ANALYSIS OF BIOPOLYMERS BY MATRIX-ASSISTED LASER-DESORPTION IONIZATION (MALDI) MASS-SPECTROMETRY [J].

BAHR, U ;

KARAS, M ;

HILLENKAMP, F .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1994, 348 (12) :783-791

[3] MATRIX-ASSISTED LASER DESORPTION IONIZATION USING A LIQUID MATRIX - FORMATION OF HIGH-MASS CLUSTER IONS FROM PROTEINS [J].

CHAN, TWD ;

COLBURN, AW ;

DERRICK, PJ .

ORGANIC MASS SPECTROMETRY, 1992, 27 (01) :53-56

[4]

CHEVRIER M, 1991, RAPID COMMUN MASS SP, V12, P611

[5]

DELL A, 1989, ANAL CARBOHYDRATES G, P217

[6] QUANTITATIVE-DETERMINATION OF BETA(1-2) CYCLIC GLUCANS BY MATRIX-ASSISTED LASER-DESORPTION MASS-SPECTROMETRY [J].

GAROZZO, D ;

SPINA, E ;

STURIALE, L ;

MONTAUDO, G ;

RIZZO, R .

RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1994, 8 (05) :358-360

[7]

HAKOMORI SI, 1964, J BIOCHEM-TOKYO, V55, P205

[8] QUANTITATIVE ASPECTS OF THE MATRIX-ASSISTED LASER-DESORPTION MASS-SPECTROMETRY OF COMPLEX OLIGOSACCHARIDES [J].

HARVEY, DJ .

RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1993, 7 (07) :614-619

[9]

JAMES CF, 1988, J AM CHEM SOC, V110, P2687

[10] MATRIX-ASSISTED LASER DESORPTION IONIZATION TIME-OF-FLIGHT MASS-SPECTROMETRY OF UNDERIVATIZED AND PERMETHYLATED GANGLIOSIDES [J].

JUHASZ, P ;

COSTELLO, CE .

JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, 1992, 3 (08) :785-796