SYNTHESIS, SEPARATION AND CHARACTERIZATION OF UNSYMMETRICALLY SUBSTITUTED PHTHALOCYANINES

被引：56

作者：

LINSSEN, TG ^{[1
]}

HANACK, M ^{[1
]}

机构：

[1] UNIV TUBINGEN,INST ORGAN CHEM,LEHRSTUHL ORGAN CHEM 2,MORGENSTELLE 18,D-72076 TUBINGEN,GERMANY

来源：

CHEMISCHE BERICHTE | 1994年 / 127卷 / 10期

关键词：

PHTHALOCYANINES; UNSYMMETRICALLY SUBSTITUTED; CHROMATOGRAPHIC SEPARATION;

D O I：

10.1002/cber.19941271030

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Unsymmetrically substitued (phthalocyaninato)nickel(II) complexes 3-7 were synthesized by statistical condensation of 4,5-dipentoxy- (2a), 4,5-diheptyl- (2b), 3,6-dihexoxy- (2c), and 3,6-diheptylphthalonitrile (2d) with 3,4,5,6-tetraphenylphthalonitrile (1) and separated by column chromatography. The obtained phthalocyanines 3-7 were characterized by UV-, IR-, and H-1-NMR spectroscopy.

引用

页码：2051 / 2057

页数：7

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