PMR ASSAY OF ESSENTIAL OILS .2. ASSAY OF METHYLSALICYLATE IN WINTERGREEN OIL

被引:5
作者
ELOBEID, HA
HASSAN, MMA
机构
[1] Dept. of Pharmaceutical Chemistry, College of Pharmacy, Riyad University, Riyad
关键词
Methyl ester; Methylsalicylate; NMR Analysis; Salicylic acid; Wintergreen Oil;
D O I
10.1080/00387017908069177
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
An NMR procedure is described for the quantitative determination of methylsalicylate as a drug entity and in wintergreen oil. For standard mixtures containing the pure drug a mean result of 99.9 + 0.75% w/w was obtained. Analysis of a wintergreen oil sample for its contents of methylsalicylate gave a mean result of 99.2 + 0.17% w/w. The results are compared with those obtained using the official procedure. © 1979 by Marcel Dekker, Inc. All Rights Reserved.
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收藏
页码:555 / 557
页数:3
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