A NEW PURIFICATION TECHNIQUE FOR ALKYL POLYGLYCOL-ETHERS AND MISCIBILITY GAPS FOR WATER CIEJ

被引:153
作者
SCHUBERT, KV [1 ]
STREY, R [1 ]
KAHLWEIT, M [1 ]
机构
[1] MAX PLANCK INST BIOPHYS CHEM,POSTFACH 2841,W-3400 GOTTINGEN,GERMANY
关键词
D O I
10.1016/0021-9797(91)90298-M
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
We report here a new procedure to purify nonionic amphiphiles (alkyl polyglycol ethers, CiEj). The method utilizes the well-known phase behavior of ternary systems of water, oil, and nonionic amphiphiles to extract simultaneously water- and oil-soluble impurities. The three-phase extraction technique (denoted as 3PHEX) is easy to apply and demonstrated to yield reproducible miscibility gaps of binary water-nonionic amphiphile mixtures. The critical temperatures and compositions for amphiphiles of varying chain length, ranging from C6E3 to C12E6, are given. © 1991.
引用
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页码:21 / 29
页数:9
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