GLASS-CAPILLARY COLUMNS IN THE GAS-CHROMATOGRAPHIC SEPARATION OF AROMATIC-AMINES .1.

被引：11

作者：

OLUFSEN, B

机构：

[1] Central Institute for Industrial Research, Blindern

来源：

JOURNAL OF CHROMATOGRAPHY | 1979年 / 179卷 / 01期

关键词：

D O I：

10.1016/S0021-9673(00)80660-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Preliminary results for the gas chromatographic analysis of aromatic amines [AA] on glass capillary columns are presented. The column is coated with a stationary phase of polyethylene glycol on a basic support, and it has been tested for polarity, adsorption and acidic properties. The separation number was evaluated, and the measurement of film thickness was discussed. Splitless injection of AA is achieved with 2-butanone as the solvent. The biological effects of AA vary from acute to chronic poisoning; some AA can give rise to cancer of the bladder or exert irritant effects on the urinary tract, and many of them induce allergies.

引用

页码：97 / 103

页数：7

共 18 条

[1]

ALEXANDER G, 1977, CHROMATOGRAPHIA, V8, P487

[2]

[Anonymous], 1978, IARC MONOGRAPHS EVAL, V16

[3] MEASUREMENT OF AVERAGE THICKNESS OF FILM OF STATIONARY PHASE IN DYNAMICALLY COATED GLASS CAPILLARY COLUMNS FOR GAS-CHROMATOGRAPHY [J].