SWINGING OF THE BENT NITROSYL LIGAND IN [CO((NO)-N-15)(TPP)] - A SOLID-STATE MOTION DETECTED BY N-15 CPMAS NMR-SPECTROSCOPY

被引：30

作者：

GROOMBRIDGE, CJ

LARKWORTHY, LF

MASON, J

机构：

[1] OPEN UNIV,DEPT CHEM,MILTON KEYNES MK7 6AA,BUCKS,ENGLAND

[2] UNIV LONDON ROYAL HOLLOWAY & BEDFORD NEW COLL,DEPT CHEM,EGHAM TW20 0EX,SURREY,ENGLAND

[3] UNIV SURREY,DEPT CHEM,GUILDFORD GU2 5XH,SURREY,ENGLAND

来源：

INORGANIC CHEMISTRY | 1993年 / 32卷 / 04期

关键词：

D O I：

10.1021/ic00056a006

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

[No abstract available]

引用

页码：379 / 380

页数：2

共 15 条

[1] LIGAND-FIELD EFFECTS IN THE NUCLEAR MAGNETIC SHIELDING OF N-15 AND COBALT-59 IN BENT NITROSYL COMPLEXES OF COBALT(III) [J].

DUFFIN, PA ;

LARKWORTHY, LF ;

MASON, J ;

STEPHENS, AN ;

THOMPSON, RM .

INORGANIC CHEMISTRY, 1987, 26 (13) :2034-2040

[2] SYNTHESIS AND N-15 NUCLEAR-MAGNETIC-RESONANCE SHIFT TENSORS OF BENT NITROSYL COMPLEXES WITH N-SUBSTITUTED SALICYLIDENEIMINATE COLIGANDS - THE SHIFT TENSOR AS A CRITERION OF MNO BOND ANGLE [J].

GROOMBRIDGE, CJ ;

LARKWORTHY, LF ;

MARECAUX, A ;

POVEY, DC ;

SMITH, GW ;

MASON, J .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1992, (21) :3125-3131

[3] SOLID-STATE C-13 NMR-SPECTRA OF IRON CARBONYL-COMPLEXES - SHIELDING TENSOR AND ERROR ANALYSES [J].

HAWKES, GE ;

SALES, KD ;

LIAN, LY ;

GOBETTO, R .

PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL PHYSICAL AND ENGINEERING SCIENCES, 1989, 424 (1866) :93-111

[4] SIDEBAND INTENSITIES IN NMR-SPECTRA OF SAMPLES SPINNING AT THE MAGIC ANGLE [J].

HERZFELD, J ;

BERGER, AE .

JOURNAL OF CHEMICAL PHYSICS, 1980, 73 (12) :6021-6030

[5] N-15 NMR EVIDENCE FOR RAPID INTRAMOLECULAR INTERCONVERSION OF LINEAR AND BENT NITROSYL LIGANDS IN [RUCL(NO)2(PPH3)2](BF4), WITH OBSERVATION OF A NITROGEN-14,15 EQUILIBRIUM ISOTOPE EFFECT [J].

MASON, J ;

MINGOS, DMP ;

SHERMAN, D ;

WARDLE, RWM .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (18) :1223-1225

[6] N-15 NMR CHARACTERIZATION OF BENT AND LINEAR NITROSYL LIGANDS IN THE SOLID-STATE BY CROSS-POLARIZATION MAGIC-ANGLE-SPINNING SPECTROSCOPY OF COMPLEXES OF RUTHENIUM [J].

MASON, J ;

MINGOS, DMP ;

SCHAEFER, J ;

SHERMAN, D ;

STEJSKAL, EO .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1985, (08) :444-446

[7]

MASON J, 1987, MULTINUCLEAR NMR, P353

[8] TEMPERATURE-DEPENDENCE OF LOCAL MOTIONS IN GLASSY POLYCARBONATE FROM CARBON AND PROTON NUCLEAR MAGNETIC-RESONANCE [J].

OGARA, JF ;

JONES, AA ;

HUNG, CC ;

INGLEFIELD, PT .

MACROMOLECULES, 1985, 18 (06) :1117-1123

[9] MOLECULAR STRUCTURE OF CHLORODINITROSYLBIS(TRIPHENYLPHOSPHINE)RUTHENIUM HEXAFLUOROPHOSPHATE-BENZENE - COMPLEX HAVING LINEAR AND BENT NITROSYL GROUPS [J].

PIERPONT, CG ;

EISENBER.R .

INORGANIC CHEMISTRY, 1972, 11 (05) :1088-&

[10] THE APPLICATION OF A SIMULTANEOUS MODEL FOR MULTISITE EXCHANGE TO SOLID-STATE NMR LINESHAPES [J].

ROY, AK ;

JONES, AA ;

INGLEFIELD, PT .

JOURNAL OF MAGNETIC RESONANCE, 1985, 64 (03) :441-450

← 1 2 →