STUDIES OF ISOPROPYLATION OF AMINO-ACIDS AND AMINES BY GAS CHROMATOGRAPHY MASS SPECTROMETRY

被引：7

作者：

BLESSINGTON, B ^{[1
]}

FIAGBE, NIY ^{[1
]}

机构：

[1] UNIV BRADFORD, DEPT PHARM CHEM, BRADFORD BD7 1DP, YORKSHIRE, ENGLAND

来源：

JOURNAL OF CHROMATOGRAPHY | 1973年 / 78卷 / 02期

关键词：

Gas chromatography-mass spectrometry - Ion exchange chromatography - Isopropylation - Phenylethylamines - Tryptamines;

D O I：

10.1016/S0021-9673(73)30086-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Urinary fractions, containing amino acids, obtained by ion-exchange chromatography were derivatised by isopropylation and examined by combined gas chromatography-mass spectrometry. Common amino acids were detected, along with a pronounced peak corresponding to creatinine. Several unidentified components were found. Selected amines, related to tryptamine and phenylethylamine, were derivatised by isopropylation and their yields (absolute and relative) and gas chromatographic-mass spectrometric characteristics were recorded. © Elsevier Scientific Publishing Company, Amsterdam.

引用

页码：343 / 347

页数：5

共 14 条

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[8] SCREENING FOR METABOLIC DISORDERS USING GAS-LIQUID CHROMATOGRAPHY, MASS SPECTROMETRY, AND COMPUTER TECHNIQUE
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[10] EVALUATION OF GAS CHROMATOGRAPHIC ANALYSIS OF PLASMA AMINO ACIDS
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FARMER, RW
FABRE, LF
[J]. JOURNAL OF CHROMATOGRAPHY, 1971, 55 (02): : 281 - +

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