DETERMINATION OF LINKAGE POSITIONS IN PERACETYLATED (METHYL) XYLO-OLIGOSACCHARIDES WITH FAST-ATOM-BOMBARDMENT MASS-SPECTROMETRY

被引：9

作者：

BLOKTIP, L ^{[1
]}

VANDERKERKVANHOOF, A ^{[1
]}

HEERMA, W ^{[1
]}

HAVERKAMP, J ^{[1
]}

KOVACIK, V ^{[1
]}

HIRSCH, J ^{[1
]}

机构：

[1] SLOVAK ACAD SCI, INST CHEM, CS-84238 BRATISLAVA, CZECHOSLOVAKIA

来源：

BIOLOGICAL MASS SPECTROMETRY | 1993年 / 22卷 / 08期

关键词：

D O I：

10.1002/bms.1200220809

中图分类号：

Q6 [生物物理学];

学科分类号：

071011 ;

摘要：

Distinction between the linkage types 1 --> 2, 1 --> 3 and 1 --> 4 of xylobioses can be achieved on the basis of the unimolecular decomposition spectra of the oxonium ions of the per-O-acetylated methyl glycosides. The spectra of the oxonium ions of various unbranched xylotri-, tetra- and pentaoses allow determination of the linkage position between the xylose residues. This indicates that in unbranched peracetylated xylo-oligosaccharides the linkage between the xylose residues at the non-reducing end can be determined.

引用

页码：474 / 480

页数：7

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