DENSE ENERGETIC COMPOUNDS OF C, H, N, AND O-ATOMS .3. 5-[4-NITRO-(1,2,5)OXADIAZOLYL]-5H-[1,2,3]TRIAZOLO[4,5-C][1,2,5]OXADIAZOLE

被引：33

作者：

GUNASEKARAN, A ^{[1
]}

BOYER, JH ^{[1
]}

机构：

[1] UNIV NEW ORLEANS,DEPT CHEM,NEW ORLEANS,LA 70148

来源：

HETEROATOM CHEMISTRY | 1993年 / 4卷 / 05期

关键词：

D O I：

10.1002/hc.520040519

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Diazidoazofurazan 8 was obtained from the bis-diazonium salt of diaminoazofurazan 7 by treatment with sodium azide and underwent thermolysis to 5-[4-azido-(1,2,5)oxadiazolyl]-5H-[1,2,3]triazolo[4,5-c] [1,2,5] oxadiazole 5. The corresponding amine 13 was obtained from the azide 5 by reduction with stannous chloride and was oxidized by ammonium persulfate to 5-[4-nitro-(1,2,5)oxadiazolyl]-5H-[1,2,3]triazolo[4,5-c] [1,2,5]oxadiazole 1. The azide 5 was converted to a phosphinimine 9 in a reaction with triphenylphosphine.

引用

页码：521 / 524

页数：4

共 17 条

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