MINIMIZATION OF SPIN-LATTICE RELAXATION-TIME WITH HIGHLY VISCOUS SOLVENTS FOR ACQUISITION OF NATURAL ABUNDANCE N-15 AND SI-29 NUCLEAR MAGNETIC-RESONANCE SPECTRA

被引：8

作者：

BAMMEL, BP ^{[1
]}

EVILIA, RF ^{[1
]}

机构：

[1] UNIV NEW ORLEANS,DEPT CHEM,NEW ORLEANS,LA 70148

来源：

ANALYTICAL CHEMISTRY | 1982年 / 54卷 / 08期

关键词：

D O I：

10.1021/ac00245a015

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

引用

页码：1318 / 1321

页数：4

共 20 条

[1]

BALCH AL, 1980, J AM CHEM SOC, V102, P1449

[2] SELECTION OF OPTIMUM PARAMETERS FOR PULSE FOURIER-TRANSFORM NUCLEAR MAGNETIC-RESONANCE [J].

BECKER, ED ;

FERRETTI, JA ;

GAMBHIR, PN .

ANALYTICAL CHEMISTRY, 1979, 51 (09) :1413-1420

[3] SENSITIVITY ENHANCEMENT IN N-15 NMR-SPECTROSCOPY OF LIQUIDS USING THE J CROSS-POLARIZATION TECHNIQUE [J].

BERTRAND, RD ;

MONIZ, WB ;

GARROWAY, AN ;

CHINGAS, GC .

JOURNAL OF MAGNETIC RESONANCE, 1978, 32 (03) :465-467

[4] RELAXATION EFFECTS IN NUCLEAR MAGNETIC RESONANCE ABSORPTION [J].

BLOEMBERGEN, N ;

PURCELL, EM ;

POUND, RV .

PHYSICAL REVIEW, 1948, 73 (07) :679-712

[5]

CARGIOLI JD, 1979, ANN REPORT NMR SPECT, P228

[6] QUENCHING NUCLEAR OVERHAUSER EFFECT IN NMR SPECTRA OF CARBON-13 [J].

FREEMAN, R ;

PACHLER, KGR ;

LAMAR, GN .

JOURNAL OF CHEMICAL PHYSICS, 1971, 55 (09) :4586-&

[7] APPLICATIONS OF NATURAL-ABUNDANCE NITROGEN-15 NUCLEAR MAGNETIC-RESONANCE TO LARGE BIOCHEMICALLY IMPORTANT MOLECULES [J].

GUST, D ;

MOON, RB ;

ROBERTS, JD .

PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 1975, 72 (12) :4696-4700

[8] EFFECT OF PARAMAGNETIC METAL IONS ON PROTON-DECOUPLED C-13 NMR INTENSITIES [J].

LAMAR, GN .

CHEMICAL PHYSICS LETTERS, 1971, 10 (02) :230-&

[9] COMPARISON BETWEEN 2 INERT PARAMAGNETIC RELAXATION REAGENTS [J].

LEVY, GC ;

EDLUND, U ;

HEXEM, JG .

JOURNAL OF MAGNETIC RESONANCE, 1975, 19 (02) :259-262

[10]

LEVY GC, 1979, NITROGEN 15 NUCLEAR, pCH5

← 1 2 →