SYNTHESIS OF NANOCRYSTALLINE NICKEL-ZINC FERRITE BY THE SOL-GEL METHOD

被引:153
作者
CHATTERJEE, A [1 ]
DAS, D [1 ]
PRADHAN, SK [1 ]
CHAKRAVORTY, D [1 ]
机构
[1] INDIAN ASSOC CULTIVAT SCI,CALCUTTA 700032,W BENGAL,INDIA
关键词
D O I
10.1016/0304-8853(93)90217-P
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Ni0.5Zn0.5Fe2O4 crystals having dimensions varying from 13 to 35 nm have been synthesized within a silica glass matrix by a sol-gel method. Particle sizes in the above range can be controlled by a suitable heat treatment schedule at temperatures varying from 973 to 1323 K. The coercivity values for different heat-treated samples are found to be in the range 20-95 Oe, which are significantly larger than that for samples having grain sizes of the order of a few microns. The Mossbauer spectra of the samples show the presence of ultrafine particles exhibiting superparamagnetic relaxation.
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页码:214 / 218
页数:5
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