RAPID ANALYSIS OF POLYOLEFIN ANTIOXIDANTS AND LIGHT STABILIZERS BY SUPERCRITICAL FLUID CHROMATOGRAPHY

被引:18
作者
KITHINJI, JP [1 ]
BARTLE, KD [1 ]
RAYNOR, MW [1 ]
CLIFFORD, AA [1 ]
机构
[1] UNIV LEEDS,SCH CHEM,LEEDS LS2 9JT,W YORKSHIRE,ENGLAND
关键词
Antioxidant; Light stabiliser; Rapid analysis; Supercritical fluid chromatography;
D O I
10.1039/an9901500125
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Nineteen commercial antioxidants and light stabilisers, with a wide range of relative molecular masses and boiling-points, present in polyolefins were analysed by packed column supercritical fluid chromatography on four different phases with CO2 or 10% MeOH - CO2 as the mobile phase and with UV detection. The technique is shown to yield short analysis times and sufficient resolution for a number of additives present in a given polyolefin.
引用
收藏
页码:125 / 128
页数:4
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