PROPERTIES AND BIOMEDICAL APPLICATIONS OF PACKINGS WITH HIGH-DENSITY COVERAGE OF C-18 CHEMICALLY BONDED PHASE FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND SOLID-PHASE EXTRACTION

被引:11
作者
BUSZEWSKI, B [1 ]
机构
[1] UNIV TUBINGEN,INST ORGAN CHEM,W-7400 TUBINGEN 1,GERMANY
来源
JOURNAL OF CHROMATOGRAPHY | 1991年 / 538卷 / 02期
关键词
D O I
10.1016/S0021-9673(01)88850-6
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A series of packing materials with high-density coverage of chemically bonded C18 phases (alpha-RP greater-than-or-equal-to 2.8-mu-mol/m2) for high-performance liquid chromatography (HPLC) and clean-up solid-phase extraction columns were prepared. The resulting packings were characterized by different physico-chemical methods including porosimetric and elemental analysis, cross-polarization magic angle spinning NMR and HPLC. The packings prepared were used for the purification by solid-phase extraction, isolation and determination of various analytes present in different biological samples.
引用
收藏
页码:293 / 301
页数:9
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