SYSTEM FOR SIMULTANEOUS DETERMINATION OF AS, SB, AND SE BY HYDRIDE GENERATION AND INDUCTIVELY COUPLED PLASMA OPTICAL-EMISSION SPECTROMETRY

被引:19
作者
PYEN, GS [1 ]
BROWNER, RF [1 ]
机构
[1] GEORGIA INST TECHNOL,SCH CHEM,ATLANTA,GA 30332
关键词
ANTIMONY AND ALLOYS - Spectroscopic Analysis - SELENIUM - Spectroscopic Analysis - SPECTROSCOPY; EMISSION - Applications - WATER ANALYSIS - Spectroscopic Analysis - WATER SUPPLY - Water Quality;
D O I
10.1366/0003702884428158
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A simple three-channel system for simultaneous determination of As, Se, and Sb by hydride generation and ICP emission spectrometry is described. The device is based on the use of simple, low-resolution prism monochromators for spectral line isolation, together with interference filters for general background reduction. Detection limits are found to be 1. 0 mu g/L, 1. 3 mu g/L, and 2. 4 mu g/L, respectively, for As, Se, and Sb. Interference studies show no significant problems for a large number of elements. Use of the method for the analysis of Standard Reference Water Samples showed generally good agreement with round-robin data.
引用
收藏
页码:262 / 266
页数:5
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