CORRECTION FOR ANISOTROPIC OFF-RESONANCE DECOUPLING EFFECTS IN CPMAS OF MODERATE SUSCEPTIBILITY MATERIALS

被引:11
作者
PRATUM, TK
机构
[1] Department of Chemistry, University of Washington, Seattle
关键词
D O I
10.1016/0009-2614(90)85405-2
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A simple decoupling method is presented which partially corrects for anisotropic off-resonance decoupling effects in magic-angle-spinning NMR spectra (CPMAS) of magnetically inhomogeneous materials. This scheme is both simpler, and more effective than previously proposed broad band decoupling methods, and is applicable to 13C CPMAS of soils and related materials. © 1990.
引用
收藏
页码:291 / 294
页数:4
相关论文
共 10 条
[1]   SPIN SPIN AND SPIN-LATTICE CONTRIBUTIONS TO THE ROTATING FRAME RELAXATION OF C-13 IN L-ALANINE [J].
AKASAKA, K ;
GANAPATHY, S ;
MCDOWELL, CA ;
NAITO, A .
JOURNAL OF CHEMICAL PHYSICS, 1983, 78 (06) :3567-3572
[2]   RESOLUTION LIMITS IN MAGIC-ANGLE ROTATION NMR-SPECTRA OF POLYCRYSTALLINE SOLIDS [J].
ALLA, M ;
LIPPMAA, E .
CHEMICAL PHYSICS LETTERS, 1982, 87 (01) :30-33
[3]   EFFECTS OF MACROSCOPIC SPINNING UPON LINEWIDTH OF NMR SIGNALS OF LIQUID IN MAGNETICALLY INHOMOGENEOUS SYSTEMS [J].
DOSKOCILOVA, D ;
TAO, DD ;
SCHNEIDER, B .
CZECHOSLOVAK JOURNAL OF PHYSICS, 1975, B 25 (02) :202-209
[4]   NMR IN ROTATING SOLIDS [J].
MARICQ, MM ;
WAUGH, JS .
JOURNAL OF CHEMICAL PHYSICS, 1979, 70 (07) :3300-3316
[5]  
MULLINS CE, 1977, J SOIL SCI, V28, P233
[6]  
PRATUM TK, IN PRESS J MAGN RESO
[7]   BROAD-BAND HETERONUCLEAR DECOUPLING IN THE PRESENCE OF HOMONUCLEAR DIPOLAR AND QUADRUPOLAR INTERACTIONS [J].
SCHENKER, KV ;
SUTER, D ;
PINES, A .
JOURNAL OF MAGNETIC RESONANCE, 1987, 73 (01) :99-113
[8]   DATA ACQUISITION AND PROCESSING - A SYSTEMS-APPROACH [J].
STERNIN, E .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1985, 56 (11) :2043-2049
[9]   BROAD-BAND HETERONUCLEAR SPIN DECOUPLING IN SOLIDS [J].
SUTER, D ;
PINES, A ;
LEE, JH ;
DROBNY, G .
CHEMICAL PHYSICS LETTERS, 1988, 144 (04) :324-327
[10]   RESOLUTION IN C-13 NMR OF ORGANIC-SOLIDS USING HIGH-POWER PROTON DECOUPLING AND MAGIC-ANGLE SAMPLE SPINNING [J].
VANDERHART, DL ;
EARL, WL ;
GARROWAY, AN .
JOURNAL OF MAGNETIC RESONANCE, 1981, 44 (02) :361-401