PROTON-ENHANCED C-13 RESONANCE IN HELIUM-COOLED PROBE - CHEMICAL SHIELDING TENSOR OF BENZENE

被引:54
作者
LINDER, M
HOHENER, A
ERNST, RR
机构
[1] Laboratorium für Physikalische Chemie, Eidgenössische Technische Hochschule
关键词
D O I
10.1016/0022-2364(79)90061-1
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The design of a helium-cooled low-temperature probe assembly for proton-enhanced carbon-13 resonance is described. As an application, the chemical shielding tensor of nonrotating benzene is measured. The principal values of the chemical shift tensor found are σ11 = -88.2, σ22 = -12.0, and σ33 =127.7 ppm with respect to liquid benzene. © 1979.
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页码:379 / 386
页数:8
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