DETERMINATION OF 3-CHLOROPROPANE-1,2-DIOL IN LIQUID HYDROLYZED VEGETABLE PROTEINS BY CAPILLARY GAS-CHROMATOGRAPHY WITH FLAME IONIZATION DETECTION

被引：32

作者：

PLANTINGA, WJ ^{[1
]}

VANTOORN, WG ^{[1
]}

VANDERSTEGEN, GHD ^{[1
]}

机构：

[1] KONINKLIJKE DOUWE EGBERTS BV,RES & DEV,KEULSEKADE 143,POB 2,3500 CA UTRECHT,NETHERLANDS

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 555卷 / 1-2期

关键词：

D O I：

10.1016/S0021-9673(01)87196-X

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

An improved method for determination of 3-chloropropane-1,2-diol in liquid hydrolysed vegetable proteins using capillary gas chromatography with flame ionization detection is presented. A phenylboronic acid derivative was prepared and extracted with hexane. The identity of the derivative was confirmed by gas chromatography-mass spectrometry. The method showed a standard deviation of 0.019 ppm and a repeatability of 0.05 ppm at a level of 0.84 ppm. The limit of detection was 0.2 ppm.

引用

页码：311 / 314

页数：4

共 3 条

[1] DETERMINATION OF RESIDUAL EPICHLOROHYDRIN AND 3-CHLOROPROPANEDIOL IN WATER BY GAS-CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION [J].

PESSELMAN, RL ;

FEIT, MJ .

JOURNAL OF CHROMATOGRAPHY, 1988, 439 (02) :448-452

[2] GAS-LIQUID-CHROMATOGRAPHY OF 3-CHLOROPROPANEDIOL [J].

RODMAN, LE ;

ROSS, RD .

JOURNAL OF CHROMATOGRAPHY, 1986, 369 (01) :97-103

[3] ANALYTICAL ENANTIOMER SEPARATION OF ALIPHATIC DIOLS AS BORONATES AND ACETALS BY COMPLEXATION GAS-CHROMATOGRAPHY [J].

SCHURIG, V ;

WISTUBA, D .

TETRAHEDRON LETTERS, 1984, 25 (49) :5633-5636

← 1 →