诺丽籽的化学成分(英文)

被引:27
作者
杨小龙 [1 ,2 ]
蒋孟圆 [1 ,2 ]
谢坤龙 [3 ]
刘吉开 [1 ]
机构
[1] 中国科学院昆明植物研究所植物化学与西部植物资源持续利用国家重点实验室
[2] 中国科学院研究生院
[3] 越南谢氏生物技术有限公司
关键词
诺丽; 黄酮; 三萜; 木脂素; 环烯醚萜; 蒽醌;
D O I
暂无
中图分类号
R284.1 [化学分析与鉴定];
学科分类号
100804 [中药化学];
摘要
目的:研究诺丽籽化学成分。方法:利用硅胶柱层析、反相RP-18、半制备薄层层析和凝胶柱层析对诺丽籽进行分离纯化,借助光谱学手段鉴定其结构。结果:分离得到20个已知化合物:胡萝卜甾醇(1),乌苏酸(2),19-羟基-乌苏酸(3),1,5,15-trimethylmorindol(4),5,15-dimethyl-morindol(5),东莨菪亭(6),3,3'-双二甲基松脂素(7),3,4,3'4'-四羟基-9,7'α-过氧化木脂素-7α,9'-丁内酯(8),americanin D(9),americanin A(10),americanin(11),isoprincepin(12),去乙酰车叶草苷酸(13),落干酸(14),车叶草苷酸(15),rhodolatouside(16),芦丁(17),4-乙基-2羟基-丁二酸(18),5-羟甲基-2-呋喃甲醛(19),3-甲基丁基-3-烯基海藻糖(20)。结论:化合物9、11、14、16和18首次从该植物中分离得到。
引用
收藏
页码:119 / 122
页数:4
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