1-11C.

被引：3

作者：

Takahashi, Toshihiro ^{[1
]}

Ido, Tatsuo ^{[1
]}

Iwata, Ren ^{[1
]}

Hatano, Kentaro ^{[1
]}

Nakanishi, Hiroaki ^{[1
]}

Shinohara, Makoto ^{[1
]}

IIda, Shigenori ^{[1
]}

机构：

[1] Tohoku Univ, Sendai, Jpn, Tohoku Univ, Sendai, Jpn

来源：

International journal of radiation applications and instrumentation. Part A, Applied radiation and isotopes | 1988年 / 39卷 / 07期

关键词：

BIOMEDICAL ENGINEERING;

D O I：

10.1016/0883-2889(88)90054-8

中图分类号：

学科分类号：

摘要：

To accommodate the increasing need for left bracket 1-**1**1C right bracket fatty acids for use in routine medical studies and the large amounts of radioactivity required, a more advanced automated synthesis system for the preparation of left bracket 1-**1**1C right bracket fatty acids has been constructed. The synthesis of left bracket 1-**1**1C right bracket fatty acids has been completely automated using a new separation unit (isobaric Sepaltor) for the extraction procedure, which had caused some difficulties with automation. The yield of left bracket 1-**1**1C right bracket palmitic acid was 20-30 mCi, and that of 3-methyl left bracket 1-**1**1C right bracket heptadecanoic acid was 2-7 mCi. The time required for the synthesis was less than 30 min from the start of the **1**1CO//2 trapping. This system has been used for more than 20 preparations of left bracket 1-**1**1C right bracket palmitic acid and more than 20 preparations of 3-methyl left bracket 1-**1**1C right bracket heptadecanoic acid.

引用

页码：659 / 665