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Keggin型磷钼杂多蓝的制备新方法——射频氢等离子体固相还原法
被引：3
作者：
李洋
储伟
陈慕华
机构：
[1] 四川大学化工学院
来源：
关键词：
磷钼杂多蓝;
射频氢等离子体;
固相还原;
Keggin结构;
质子化;
D O I：
暂无
中图分类号：
O614.612 [];
学科分类号：
摘要：
A novel glow discharge plasma solid-state reduction route was developed to synthesize molybdophosphoric heteropoly blues(MB). The glow discharge plasma played a role of activating hydrogen mole-cules and generated a lot of active species which rapidly induced molybdophosphoric heteropoly acid(PMo12) to form four-electron MB within several minutes. Analyses of the heteropoly blues via UV-Vis, FTIR, XRD and Py-IR confirmed that the materials retained not only the similar Keggin structures of their oxidized parents, but also exhibited more surface acidity due to protonation.
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页码：771 / 773
页数：3
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