Zn(Oxin)2·2H2O纳米晶的固相化学反应合成及表征

被引:8
作者
李道华
忻新泉
机构
[1] 西昌学院
[2] 南京大学配位化学研究所
[3] 配位化学国家重点实验室 西昌
[4] 南京
关键词
Zn(Oxin)2·2H2O(8-羟基喹啉锌); 纳米晶; 固相化学反应; 合成与表征;
D O I
暂无
中图分类号
O614 [金属元素及其化合物];
学科分类号
070301 ; 081704 ;
摘要
Nanocrystalline Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) was synthesized at near ambient temperature by solid state chemical reaction. Phases, particle sizes and morphology of the prepared nanocrystallite were characterized by Powder X-ray diffraction (XRD) and transmission electron microscopy(TEM). The results showed that the crystallite product had an average size about 30 nm. The effects of a series of reaction conditions on the synthesis of Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) by solid state reaction were studied.
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页码:873 / 878+752 +752
页数:7
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