人尿中美托拉宗的液相色谱-质谱研究

被引：2

作者：

秦旸

张建丽

机构：

[1] 国家体育总局运动医学研究所兴奋剂检测中心

来源：

分析测试学报 | 2007年 / S1期

关键词：

D O I：

暂无

中图分类号：

R87 [运动医学];

学科分类号：

100911 [运动医学];

摘要：

A sensitive and reliable procedure for analysis of metolazone in human urine by HPLC-MS was describes.The extraction recovery of liquid-liquid extraction (LLE) at various pH were studied.The detection limit of the compound was below 0.2ng at absolute amount.It is suitable for metolazone screening and confirmation in doping control.

引用

页码：69 / 70+74 +74

页数：3

共 3 条

[1]

兴奋剂中利尿剂的检测方法 [J].

秦旸 ;

朱绍棠 ;

张长久 .

分析测试学报, 2001, (02) :82-86

[2]

Application of high-performance liquid chromatography–mass spectrometry to detection of diuretics in human urine[J] Y. Qin;X.B. Wang;C. Wang;M. Zhao;M.T. Wu;Y.X. Xu;S.Q. Peng Journal of Chromatography B 2003,

[3]

Screening for 18 diuretics and probenecid in doping analysis by liquid chromatography–tandem mass spectrometry[J] K.Deventer;F. T.Delbeke;K.Roels;P.Van Eenoo Biomed. Chromatogr. 2002,

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