香樟木质部挥发性成分的SPME-GC/MS分析

被引:11
作者
李权 [1 ]
王晓娴 [1 ]
林金国 [1 ]
江茂生 [2 ]
初雷霞 [2 ]
机构
[1] 福建农林大学材料工程学院
[2] 福建农林大学生命科学学院
关键词
香樟; 固相微萃取; 挥发性成分; 气相色谱-质谱(GC/MS);
D O I
暂无
中图分类号
O657.63 [质谱分析]; TQ651.2 [];
学科分类号
070302 ; 081704 ; 0817 ;
摘要
采用固相微萃取技术(SPME)吸附香樟木质部挥发性成分,结合气相色谱-质谱(GC/MS)进行化学成分的分离和鉴定,同时比较不同色谱柱对分离效果的影响。结果表明:采用弱极性DB-5MS色谱柱共分离出51个组分,解析出43种挥发性成分,占总峰面积的97.04%,分离效果和所得的峰形较好于DB-WAXetr色谱柱。鉴定出含量较高的成分有:左旋-α-蒎烯(4.57%)、莰烯(2.14%),双环[3.1.0]-4-甲基-1-异丙基-2-己烯(4.16%)、β-蒎烯(2.3%)、邻异丙基甲苯(2.15%)、D-柠檬烯(7.49%)、桉叶油醇(13.85%)、樟脑(38.71%)、(R)-4-萜品醇(1.74%)、α-松油醇(2.40%)、黄樟素(2.96%)、α-荜澄茄油烯(4.36%)、1-石竹烯(1.92%)等。该方法可为香樟材在医药、食品和化学工业等方面的进一步开发和利用提供参考。
引用
收藏
页码:555 / 562
页数:8
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