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中药复方中柴胡皂甙A和D的LC/MS/MS研究
被引：17
作者：
刘密新
吴筑平
杨成对
刘国文
机构：
[1] 清华大学分析中心! 北京
[2] 清华大学分析中心!北京
来源：
关键词：
柴胡皂甙;
LC/MS/MS;
选择离子检测;
MS;
标准品;
中药复方;
D O I：
暂无
中图分类号：
O657.6 [];
学科分类号：
070302 ;
081704 ;
摘要：
To study Saikosaponins in a Chinese traditional compound medicine by LC/MS. Saikosaponin A and D, which were the bioactive components of Bupleurum falcatum L., were not found in the medicine. And three isomeric compounds of Saikosaponin A and D were detected instead. Saikosaponin A and D were found have turned into two other isomers after treated by acid water, but keep unchanged when treated by neutral water. Two of the isomeric compounds which found in the Compound medicine were determined as Saikosaponin B1 and B2 . This work is helpful for quality control of the medicine and also is useful for supervising the procedures of manufacture.
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页码：77 / 78
页数：2
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